Suggest structures from IR spectra

Unknown U has formula C₃H₆O, a strong 1715 cm⁻¹ band and no broad O–H absorption.

  • GCE A-Level H3 Chemistry 9813-2027
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Learning objectives

  • Suggest structures from IR spectra

Constrain an unknown

Unknown U has formula C₃H₆O, a strong 1715 cm⁻¹ band and no broad O–H absorption.

The formula permits one degree of unsaturation; the carbonyl accounts for it and propanone is consistent, but the whole evidence set must be checked.

A deduction is a tested candidate

Structure deduction combines molecular formula, characteristic bands and important absences to propose a structure.

A consistent candidate predicts every supplied feature; IR alone may leave constitutional isomers unresolved.

Formula first, spectrum second

Use the formula to restrict atoms and unsaturation, then assign understanding check bands. Reject candidates that require an absent band.

For C2H6O, broad 3200–3600 cm⁻¹ and no 1700 cm⁻¹ supports ethanol over methoxymethane only when C–O/fingerprint evidence is also considered.

Deduce C₃H₆O

The 1715 cm⁻¹ band supports C=O and no broad O–H excludes an alcohol. Absence of aldehydic C–H evidence favours propanone over propanal.

State propanone as the best supplied candidate, not as a conclusion from 1715 cm⁻¹ alone.

Try this

Use formula C₃H₆O and the fixed spectrum to choose propanone or propanal.

Check your answer

Choose propanone only after using C=O presence and aldehydic-feature absence; acknowledge IR resolution limits.

Choose ethanol or methoxymethane

C2H6O shows broad 3340 cm⁻¹ and no 1700–1750 cm⁻¹ band.

The two candidates are ethanol, CH₃CH₂OH, and methoxymethane, CH₃OCH₃.

Try this

Select the consistent structure and cite one present and one absent feature.

Check your answer

Ethanol. The broad 3340 cm⁻¹ O–H band is present, and methoxymethane has no O–H bond. The absent 1700–1750 cm⁻¹ band is consistent with both candidates, because neither contains C=O, so it cannot be the deciding feature.

Test an ester candidate

C4H8O2 shows strong 1740 cm⁻¹, strong 1240 cm⁻¹ and no broad O–H.

Consider more than one functional-group class that fits C4H8O2, and use the absent band as well as the present ones.

Try this

Propose one structure and predict two bands it should contain.

Check your answer

An ester fits: for example ethyl ethanoate, with C=O near 1740 and C–O near 1240 cm⁻¹. Butanoic acid also has formula C4H8O2 but would show a very broad 2500–3300 cm⁻¹ O–H band, which is absent. IR alone does not pick out which ester isomer it is.

Do not name from the tallest peak

The base peak concept belongs to mass spectrometry; an IR trough's intensity does not uniquely name a molecule.

Deduction requires formula plus multiple positive/negative constraints.

Try this

Better reasoning: “The deepest 1715 cm⁻¹ trough proves propanone.”

Check your answer

Replace proof with carbonyl support, then add formula and absence evidence before proposing propanone.

Deduce, predict, falsify

After the check questions, deduce the C₃H₆O₂ structure without notes. Return later for a different C₄H₈O question.

Try this next: predict bands from a known structure.

Try this

Write a three-column evidence table for U: observation, inference, candidates rejected.

Check your answer

A strong answer should include formula, 1715 cm⁻¹ C=O, absent O–H and an explicit test of propanone against propanal.

Suggest structures from IR spectra scientific representation

Two separate transmittance traces run from 4000 to 500 cm⁻¹. Unknown U, C3H6O, has a weak band near 2970 and a strong trough at 1715, with no broad trough from 2500 to 3600. Unknown V, C4H8O2, has a weak band near 2985 and strong troughs at 1740 and 1240, with no broad trough from 2500 to 3600.

About 5 minutes

Key visual: Suggest structures from IR spectra. Two fixed unknown spectra plus formula panels allow a genuine constraint-and-falsification deduction.
Suggest structures from IR spectra authored spectrumTwo separate transmittance traces run from 4000 to 500 cm⁻¹. Unknown U, C3H6O, has a weak band near 2970 and a strong trough at 1715, with no broad trough from 2500 to 3600. Unknown V, C4H8O2, has a weak band near 2985 and strong troughs at 1740 and 1240, with no broad trough from 2500 to 3600.transmittance / %wavenumber / cm⁻¹ (high → low)4000500U: below 3000U: 1715 strongV: below 3000V: 1740 strongV: 1240 strongUnknown U, C₃H₆OUnknown V, C₄H₈O₂
Unknown spectra and candidate checks
Unknown / formulaExact band / cm⁻¹Strength / widthCandidate comparisonExplicit absence
U / C3H6O1715strong, narrowpropanone supported; propanal would require aldehydic C–Hno broad O–H; no aldehydic C–H
V / C4H8O21740; 1240strong; strongester supported; acid would require broad O–Hno broad O–H

Text alternative: Two separate transmittance traces run from 4000 to 500 cm⁻¹. Unknown U, C3H6O, has a weak band near 2970 and a strong trough at 1715, with no broad trough from 2500 to 3600. Unknown V, C4H8O2, has a weak band near 2985 and strong troughs at 1740 and 1240, with no broad trough from 2500 to 3600.