Variable Oxidation States and Redox Systems

Learn and apply Variable Oxidation States and Redox Systems in the published Chemistry course sequence.

  • GCE A-Level H2 Chemistry 9476-2027
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Variable Oxidation States and Redox Systems: Orientation

This lesson focuses on the redox systems that actually show up in structured and data questions: Fe³⁺/Fe²⁺, acidified permanganate, and acidified dichromate, including the half-equations and colour-change marks.

This chapter depends on periodic trends, so keep The Periodic Table (A Level) nearby and use the Transition Elements hub for the full sequence.

This page is really testing:

  • Can you recall and apply the standard acidic half-equations without missing H⁺ and H₂O?
  • Can you write colour-change observations precisely for Mn and Cr oxidising agents?
  • Can you combine half-equations into a balanced ionic equation with correct electrons and charges?

Definitions (Must Know)

A. Variable oxidation states

Many transition elements show more than one stable oxidation state because the 3d and 4s electrons are similar in energy and can both be involved in bonding.

B. Key oxidising agents (acidic conditions)

  • MnO₄⁻ (permanganate): purple → Mn²⁺ very pale (acidic)
  • Cr₂O₇²⁻ (dichromate): orange → Cr³⁺ green (acidic)

Detailed Explanations

A. Why variable oxidation states happen (what to write)

Write something like:

  • “The 3d and 4s orbitals are close in energy, so different numbers of electrons can be lost or shared, giving multiple oxidation states.”

Because 3d and 4s orbitals are close in energy, therefore more than one number of electrons can be involved in bonding, giving multiple stable oxidation states.

B. Core redox half-equations (acidic conditions)

Permanganate reduction (acidic): MnO₄⁻ + 8H⁺ + 5e⁻ → Mn²⁺ + 4H₂O

Dichromate reduction (acidic): Cr₂O₇²⁻ + 14H⁺ + 6e⁻ → 2Cr³⁺ + 7H₂O

Iron redox: Fe³⁺ + e⁻ → Fe²⁺ Fe²⁺ → Fe³⁺ + e⁻

C. Workflow: combining half-equations in acidic solution (exam method)

  1. Write both half-equations.
  2. Multiply to balance electrons.
  3. Add and cancel electrons (and any common species).
  4. Check atoms and charge.

Mini example: To combine permanganate reduction (5e−) with Fe²⁺ → Fe³⁺ + e⁻, multiply the iron oxidation by 5 so 5 electrons cancel.

D. Worked method for redox-identification questions

When a question gives observations plus reagents, this route is reliable:

  1. Identify reagent conditions first (acidified permanganate/dichromate means acidic half-equations).
  2. Write the observation line (purple to colourless, orange to green).
  3. Name which species is reduced (oxidising agent) and which is oxidised.
  4. Add balanced half-equation(s) only if asked.

E. Predicting likely oxidation states from a configuration

Remove 4s electrons first, then consider how many 3d electrons can be removed to reach a relatively stable configuration. Treat the result as a prediction, not proof: supplied chemical evidence controls which oxidation states are actually stable. For example, [Ar]3d^54s^2 readily suggests +2 and +3 because both ions retain incomplete d subshells.

F. Using E⦵ values

Write both couples as reductions. The more positive reduction potential remains as reduction; reverse the other half-equation for oxidation. A positive E⦵_cell predicts feasibility for the combined equation as written under standard conditions. Kinetic barriers and non-standard conditions remain separate limitations.

Worked Examples

Modelled example 1

Permanganate Reduction in Acid

Core

Problem

Write the half-equation for MnO₄⁻ being reduced to Mn²⁺ in acidic solution.
Study the worked solution
  1. Balance oxygen and hydrogen

    Method

    Add four waters to products and eight protons to reactants.

    Reason

    This balances four O and eight H atoms in acidic medium.

    Working

    MnO₄⁻ + 8H⁺ → Mn²⁺ + 4H₂O.
  2. Balance charge

    Method

    Add five electrons to the reactants.

    Reason

    Left charge becomes -1 + 8-5 = +2, matching Mn²⁺.

    Working

    MnO₄⁻ + 8H⁺ + 5e⁻ → Mn²⁺ + 4H₂O.

Common misconception 2

Dichromate Reduction Colour

Find and correct the mistake

Learner claim

A learner says reducing acidified dichromate(VI) to Cr³⁺ changes green to orange. Correct the direction.

Match colour to oxidation state

Cr₂O₇²⁻
Cr³⁺

View solution step by step
  1. Identify reactant colour

    Method

    Start with orange dichromate(VI).

    Reason

    The species being reduced is Cr₂O₇²⁻.

    Working

    Orange.
  2. Identify product colour

    Method

    End with green chromium(III).

    Reason

    Reduction forms Cr³⁺.

    Working

    Orange → green.

Challenge 3

Permanganate Oxidising Iron(II)

Minimal support

Equation transfer

Use half-equations to show MnO₄⁻ oxidising Fe²⁺ to Fe³⁺ in acidic solution.

Equalise and cancel electrons

Fe half-equation multiplier
Iron product

Hints

Hint 1: oxidation
Fe²⁺ → Fe³⁺ + e⁻.
Hint 2: scale
The permanganate half-equation consumes five electrons.
View solution step by step
  1. Scale iron oxidation

    Method

    Multiply Fe²⁺ → Fe³⁺ + e⁻ by five.

    Reason

    This supplies five electrons.

    Working

    5Fe²⁺ → 5Fe³⁺ + 5e⁻.
  2. Add and cancel

    Method

    Combine with permanganate reduction and remove electrons.

    Reason

    Transferred electrons do not appear in the overall ionic equation.

    Working

    MnO₄⁻ + 8H⁺ + 5Fe²⁺ → Mn²⁺ + 4H₂O + 5Fe³⁺.

Mind Stretchers

Mind stretcher 1Extension

In acidic solution, Cr₂O₇²⁻ oxidises I⁻ to I₂. Using the half-equations, write the balanced overall ionic equation.

Show Hint

Use the acidic dichromate reduction half-equation and scale the iodide oxidation half-equation to six electrons.

Show Answer

Mark scheme:

  • Reduction (dichromate): Cr₂O₇²⁻ + 14H⁺ + 6e⁻ → 2Cr³⁺ + 7H₂O
  • Oxidation (iodide): 2I⁻ → I₂ + 2e⁻ (×3)
  • Overall: Cr₂O₇²⁻ + 14H⁺ + 6I⁻ → 2Cr³⁺ + 7H₂O + 3I₂

Mind stretcher 2: Using electrode potentials with a transition-metal coupleExtension

Question. Standard reduction potentials are E⦵(Fe³⁺/Fe²⁺) = +0.77 V and E⦵(I₂/I⁻) = +0.54 V. Predict whether Fe³⁺ oxidises I⁻ under standard conditions and write the equation.

Show Hint

The more positive reduction potential stays as reduction; reverse the other half-equation and subtract.

Show Answer

The more positive iron couple is reduced, so Fe³⁺ gains electrons while I⁻ is oxidised. E⦵_cell = 0.77-0.54 = +0.23 V, so the reaction is feasible as written under standard conditions: 2Fe³⁺ + 2I⁻ → 2Fe²⁺ + I₂